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Pace Analytical Services,Inc. <br /> aceAnalytical e 1241 Bellevue Street-Suite 9 <br /> Green Bay,WI 54302 <br /> wm 'com (920)469-2436 <br /> QUALIFIERS <br /> Project: KLAHN AGGR.SITE <br /> Pace Project No.: 40130276 <br /> DEFINITIONS <br /> DF-Dilution Factor, if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. <br /> ND-Not Detected at or above LOD. <br /> J-Estimated concentration at or above the LOD and below the LOQ. <br /> LOD-Limit of Detection adjusted for dilution factor and percent moisture. <br /> LOQ-Limit of Quantitation adjusted for dilution factor and percent moisture. <br /> S-Surrogate <br /> 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is <br /> a combined concentration. <br /> Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate%recovery and RPD values. <br /> LCS(D)-Laboratory Control Sample(Duplicate) <br /> MS(D)-Matrix Spike(Duplicate) <br /> DUP-Sample Duplicate <br /> RPD-Relative Percent Difference <br /> NC-Not Calculable. <br /> SG-Silica Gel-Clean-Up <br /> U-Indicates the compound was analyzed for,but not detected at or above the adjusted LOD. <br /> N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for <br /> each analyte is a combined concentration. <br /> Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. <br /> TNI-The NELAC Institute. <br /> LABORATORIES <br /> PASI-G Pace Analytical Services-Green Bay <br /> PASI-I Pace Analytical Services-Indianapolis <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced,except in full, <br /> Date:04/13/2016 03:03 PM without the written consent of Pace Analytical Services,Inc.. Page 8 of 11 <br />